2,4,4,5,5-五氟-2-(三氟甲基)-1,3-恶噻戊环3,3-二氧化物合成路线 （共 5 条）
反应条件
1: With sodium carbonate in various solvent(s) T=40°C; 1 h; 2: in various solvent(s) T=160°C; Further stages.;
参考文献
Uematsu, Nobuyuki; Hoshi, Nobuto; Koga, Takehiro; Ikeda, Masanori
Journal of Fluorine Chemistry, 2006 , vol. 127, # 8 p. 1087 - 1095
参考文献
Asahi Kasei Kabushiki Kaisha
Patent: EP1359142 A1, 2003 ;
Location in patent: Page/Page column 51 ;
反应条件
1: With cesium fluoride in various solvent(s) T=-15°C; P=750 Torr; 8 h; 2: With sodium carbonate T=210 - 225°C; 4 h;
参考文献
Thomas, Brian H.; Shafer, Gregory; Ma, Jing Ji; Tu, Ming-Hu; DesMarteau, Darryl D.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 8 p. 1231 - 1240
反应条件
3 h at 300°C under N2 driend, Na2CO3 used;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.8, page 183 - 184
Full Text Show Details
Resnick, P. R.
C.A., Deut. Offenlegungsschrift 1959143 <1968/70> 1970 , vol. 73, p. 766592
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
