2-甲基-呋喃[3,2-c]吡啶-4(5H)-酮合成路线 （共 7 条）
反应条件
(i) ClCO2Et, Et3N, acetone, (ii) aq. NaNO2, (iii) nBu3N, Ph2CH2; Multistep reaction;
参考文献
Li, Lingjun; Degardin, Melissa; Lavergne, Thomas; Malyshev, Denis A.; Dhami, Kirandeep; Ordoukhanian, Phillip; Romesberg, Floyd E.
Journal of the American Chemical Society, 2014 , vol. 136, # 3 p. 826 - 829
反应条件
acetic anhydride 1.5 h; Heating;
参考文献
Yamaguchi, Seiji; Kurosaki, Masahide; Orito, Keiko; Yokayama, Hajime; Hirai, Yoshiro; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 6 p. 1237 - 1247
反应条件
1: 94 percent / m-CPBA / CHCl3 / 15 h / Ambient temperature 2: 52 percent / Ac2O / 1.5 h / Heating View Scheme
参考文献
Yamaguchi, Seiji; Kurosaki, Masahide; Orito, Keiko; Yokayama, Hajime; Hirai, Yoshiro; Shiotani, Shunsaku
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 6 p. 1237 - 1247
反应条件
1: pyridine; piperidine / 13 h / 100 °C 2: thionyl chloride / chloroform; N,N-dimethyl-formamide / 3 h / |Reflux 3: sodium azide / 1,4-dioxane; water / 0.5 h / 5 °C 4: chloroform; diphenylether / 1 h / 230 °C View Scheme
参考文献
Li, Lingjun; Degardin, Melissa; Lavergne, Thomas; Malyshev, Denis A.; Dhami, Kirandeep; Ordoukhanian, Phillip; Romesberg, Floyd E.
Journal of the American Chemical Society, 2014 , vol. 136, # 3 p. 826 - 829
反应条件
1: sodium azide / 1,4-dioxane; water / 0.5 h / 5 °C 2: chloroform; diphenylether / 1 h / 230 °C View Scheme
参考文献
Li, Lingjun; Degardin, Melissa; Lavergne, Thomas; Malyshev, Denis A.; Dhami, Kirandeep; Ordoukhanian, Phillip; Romesberg, Floyd E.
Journal of the American Chemical Society, 2014 , vol. 136, # 3 p. 826 - 829
反应条件
1: POCl3 / Heating 2: Zn, AcOH / 8 h / Heating View Scheme
参考文献
Eloy,F.; Deryckere,A.
Journal of Heterocyclic Chemistry, 1971 , vol. 8, p. 57 - 60
反应条件
trichlorophosphate Heating;
参考文献
Eloy,F.; Deryckere,A.
Journal of Heterocyclic Chemistry, 1971 , vol. 8, p. 57 - 60
