8-甲氧基-2-苯基色原酮合成路线 （共 6 条）
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane T=0 - 80°C; 14 h; Inert atmosphere; regioselective reaction;
参考文献
Yoshida, Masahito; Fujino, Yuta; Saito, Koya; Doi, Takayuki
Tetrahedron, 2011 , vol. 67, # 51 p. 9993 - 9997
反应条件
piperidine; anhydrous iron chloride in toluene 10 h; Reflux;
参考文献
Maiti, Gourhari; Karmakar, Rajiv; Bhattacharya, Rudraksha N.; Kayal, Utpal
Tetrahedron Letters, 2011 , vol. 52, # 43 p. 5610 - 5612
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere 1.2: 1.5 h / -78 - 0 °C / Inert atmosphere 1.3: 0 °C 2.1: manganese(IV) oxide / acetone / 20 °C / Inert atmosphere 3.1: trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 14 h / 0 - 80 °C / Inert atmosphere View Scheme
参考文献
Yoshida, Masahito; Fujino, Yuta; Saito, Koya; Doi, Takayuki
Tetrahedron, 2011 , vol. 67, # 51 p. 9993 - 9997
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere 1.2: 1.5 h / -78 - 0 °C / Inert atmosphere 1.3: 0 °C 2.1: manganese(IV) oxide / acetone / 20 °C / Inert atmosphere 3.1: trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 14 h / 0 - 80 °C / Inert atmosphere View Scheme
参考文献
Yoshida, Masahito; Fujino, Yuta; Saito, Koya; Doi, Takayuki
Tetrahedron, 2011 , vol. 67, # 51 p. 9993 - 9997
反应条件
1: sodium benzoate / 180 °C 2: aqueous sodium carbonate-solution 3: potassium carbonate; acetone View Scheme
参考文献
Ahluwalia et al.
Proceedings - Indian Academy of Sciences, Section A, 1953 , # 38 p. 480,490
反应条件
potassium carbonate; acetone
参考文献
Ahluwalia et al.
Proceedings - Indian Academy of Sciences, Section A, 1953 , # 38 p. 480,490
