9,10-双(1-萘基)蒽合成路线 (共 5 条)
反应条件
1: 1-Bromonaphthalene With tert.-butyl lithium in pentane T=-78 - 20°C; 2: With indium(III) chloride in tetrahydrofuran; diethyl ether; pentane T=-78 - 20°C; 1 h; 3: 9,10-Dibromoanthracene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; diethyl ether; pentane T=70°C; 8 h; Further stages.;
参考文献
Lee, Wonhyung; Kang, Youngjin; Lee, Phil Ho
Journal of Organic Chemistry, 2008 , vol. 73, # 11 p. 4326 - 4329
反应条件
sodium hypophosphite; acetic acid; potassium iodide
参考文献
Lee, Cho Hee; Kim, Mi Jong; Han, Sang-Pil; Lee, Yoo-Soon; Kang, Sung Kwon; Song, Jae Hee; Je, Jong Tae; Oh, Hyoung-Yun; Kim, Yeong-Joon
Tetrahedron, 2010 , vol. 66, # 18 p. 3360 - 3364
参考文献
Lee, Cho Hee; Kim, Mi Jong; Han, Sang-Pil; Lee, Yoo-Soon; Kang, Sung Kwon; Song, Jae Hee; Je, Jong Tae; Oh, Hyoung-Yun; Kim, Yeong-Joon
Tetrahedron, 2010 , vol. 66, # 18 p. 3360 - 3364
反应条件
Suzuki-Miyaura reaction;
参考文献
Lee, Cho Hee; Kim, Mi Jong; Han, Sang-Pil; Lee, Yoo-Soon; Kang, Sung Kwon; Song, Jae Hee; Je, Jong Tae; Oh, Hyoung-Yun; Kim, Yeong-Joon
Tetrahedron, 2010 , vol. 66, # 18 p. 3360 - 3364
反应条件
aluminium trichloride; sodium chloride T=160°C;
参考文献
Clar et al.
Journal of the Chemical Society, 1956 , p. 2652,2655