1-甲基-4-(1-丙烯-1-基)苯合成路线 （共 16 条）
反应条件
1: para-bromotoluene With magnesium; lithium chloride in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
2: With iron (III) acetylacetonate in tetrahydrofuran
T=0°C; 0.0833333 h; Inert atmosphere;
3: diethyl allyl phosphate in tetrahydrofuran
T=0°C; 1 h; Inert atmosphere;
参考文献
Mayer, Matthias; Czaplik, Waldemar M.; Von Wangelin, Axel Jacobi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2147 - 2152
反应条件
1: para-bromotoluene With magnesium; lithium chloride in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
2: With iron (III) acetylacetonate in tetrahydrofuran
T=0°C; 0.0833333 h; Inert atmosphere;
3: ethylene,methyl acetate in tetrahydrofuran
T=0°C; 0.75 h; Inert atmosphere;
参考文献
Mayer, Matthias; Czaplik, Waldemar M.; Von Wangelin, Axel Jacobi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2147 - 2152
反应条件
1: para-bromotoluene With magnesium; lithium chloride in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
2: With iron (III) acetylacetonate in tetrahydrofuran
T=0°C; 0.0833333 h; Inert atmosphere;
3: allyl bromide in tetrahydrofuran
T=0°C; 1 h; Inert atmosphere;
参考文献
Mayer, Matthias; Czaplik, Waldemar M.; Von Wangelin, Axel Jacobi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2147 - 2152
反应条件
carbon dioxide
T=300°C; Leiten ueber Platin-Kohle;
参考文献
Lewina; Petrow
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 747,748
Chem. Zentralbl., 1938 , vol. 109, # I p. 302
反应条件
hydrogenchloride
P=20 - 27 Torr; durch Destillation und Behandeln mit Pyridin oder Chinolin;
参考文献
Klages
Chemische Berichte, 1902 , vol. 35, p. 2263
Chemische Berichte, 1905 , vol. 38, p. 913
反应条件
T=300°C; Leiten ueber Platin-Kohle;
参考文献
Lewina; Petrow
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 747,748
Chem. Zentralbl., 1938 , vol. 109, # I p. 302
