4-溴-3,5-二甲基苄醇合成路线 （共 5 条）
反应条件
sodium tetrahydroborate in tetrahydrofuran; water T=0 - 20°C; 0.5 h;
参考文献
Kawate, Tomohiko; Iwase, Noriaki; Shimizu, Motohisa; Stanley, Sarah A.; Wellington, Samantha; Kazyanskaya, Edward; Hung, Deborah T.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 22 p. 6052 - 6059
反应条件
1: With chromium(VI) oxide; acetic anhydride; acetic acid 2: With lithium aluminium tetrahydride
参考文献
Wessig, Pablo; Teubner, Janek
Synlett, 2006 , # 10 p. 1543 - 1546
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Grisdale,P.J. et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 544 - 549
反应条件
1: nBuLi / diethyl ether 2: LiAlH4 / diethyl ether View Scheme
参考文献
Grisdale,P.J. et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 544 - 549
反应条件
chromium(VI) oxide; lithium aluminium tetrahydride; sulfuric acid; acetic anhydride 1.) acetic acid, 5 deg C, 30 min, large scale; 2.) anhydrous ether, 90 min; Multistep reaction. Title compound not separated from byproducts;
参考文献
Ayer; McCaskill
Canadian Journal of Chemistry, 1981 , vol. 59, # 14 p. 2159 - 2169
