4,5-二甲基-2-苯基吡啶合成路线 (共 5 条)
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in toluene T=130°C; 48 h; Inert atmosphere;
参考文献
Ohashi, Masato; Takeda, Ippei; Ikawa, Masashi; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18018 - 18021
反应条件
ammonium acetate in formamide T=80°C; 6 h;
参考文献
Sasaki, Isabelle; Vendier, Laure; Sournia-Saquet, Alix; Lacroix, Pascal G.
European Journal of Inorganic Chemistry, 2006 , # 16 p. 3294 - 3302
反应条件
nickel in ethanol; benzene 6 h; Heating;
参考文献
Bryce, Martin R.; Reynolds, Colin D.; Hanson, Peter; Vernon, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 607 - 613
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in deuterated toluene T=130°C; 62 h; Inert atmosphere;
参考文献
Ohashi, Masato; Takeda, Ippei; Ikawa, Masashi; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18018 - 18021
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in deuterated toluene T=130°C; 23 h; Inert atmosphere;
参考文献
Ohashi, Masato; Takeda, Ippei; Ikawa, Masashi; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18018 - 18021