1: With titanium(IV) isopropylate in tetrahydrofuran; diethyl ether T=20°C; 1 h; 2: With boron trifluoride diethyl etherate in tetrahydrofuran; diethyl ether 1 h; 3: With sodium hydroxide; water in tetrahydrofuran; diethyl ether
参考文献
ABBOTT GMBH and CO. KG
Patent: WO2006/40179 A1, 2006 ;
Location in patent: Page/Page column 97 ;
WO 2006/040179 A1
1: With titanium(IV) isopropylate in tetrahydrofuran T=20°C; 1 h; 2: With boron trifluoride diethyl etherate in diethyl ether T=20°C; 0.5 h; 3: With sodium hydroxide Further stages.;
参考文献
Bertus; Szymoniak
Chemical Communications, 2001 , # 18 p. 1792 - 1793