[2-(烯丙氧基)苯基]胺合成路线 (共 13 条)
反应条件
hydrogenchloride; tin(ll) chloride in ethanol; water
参考文献
Jasch, Hannelore; Landais, Yannick; Heinrich, Markus R.
Chemistry - A European Journal, 2013 , vol. 19, # 26 p. 8411 - 8416
反应条件
hydrogenchloride in water 4 h; Reflux;
参考文献
Siqueira, Fernanda A.; Taylor, Jason G.; Correia, Carlos Roque D.
Tetrahedron Letters, 2010 , vol. 51, # 16 p. 2102 - 2105
反应条件
MoO2[S2CNEt2]2; phenyl silane in toluene T=100°C; 5 h;
参考文献
Maddani, Mahagundappa R.; Moorthy, Saravana K.; Prabhu, Kandikere R.
Tetrahedron, 2010 , vol. 66, # 1 p. 329 - 333
反应条件
1: potassium carbonate; acetone 2: aqueous hydrochloric acid View Scheme
参考文献
Xia, Zhonghua; Huang, Jinbo; He, Yimiao; Zhao, Jiaji; Lei, Jian; Zhu, Qiang
Organic Letters, 2014 , vol. 16, # 9 p. 2546 - 2549
反应条件
1: With potassium carbonate in acetone 20 h; Reflux; 2: With hydrogenchloride in dichloromethane; water 1 h;
参考文献
Wang, Renchao; Xu, Jiaxi
Arkivoc, 2010 , vol. 2010, # 9 p. 293 - 299
反应条件
1: ethyl acetate / 4 h / 0 - 20 °C 2: potassium carbonate / acetone / 20 h / 0 °C / |Reflux 3: hydrogenchloride / water / 4 h / |Reflux View Scheme
参考文献
Xia, Zhonghua; Huang, Jinbo; He, Yimiao; Zhao, Jiaji; Lei, Jian; Zhu, Qiang
Organic Letters, 2014 , vol. 16, # 9 p. 2546 - 2549
反应条件
1: potassium carbonate / acetone / |Reflux 2: tin(ll) chloride; hydrogenchloride / water; ethanol View Scheme
参考文献
Jasch, Hannelore; Landais, Yannick; Heinrich, Markus R.
Chemistry - A European Journal, 2013 , vol. 19, # 26 p. 8411 - 8416
参考文献
Tiffany
Journal of the American Chemical Society, 1948 , vol. 70, p. 592
反应条件
1: 53 percent / tert-BuOK / dimethylsulfoxide / 1 h / Ambient temperature
2: 1.) aq. HCl, NaNO2, 2.) NaN3
3: 81 percent / CDCl3 / 10 h / 150 °C
View Scheme
参考文献
Smith, Peter A. S.; Chou, Shang-shing Peter
Journal of Organic Chemistry, 1981 , vol. 46, # 20 p. 3970 - 3977
反应条件
1.1: sodium nitrite / water / 0.5 h / 0 °C
2.1: iron sulphate heptahydrate; sodium acetate; acetic acid; nitrogen(II) oxide / water; dimethyl sulfoxide / 1 h / |Inert atmosphere
2.2: 0.33 h / |Inert atmosphere
View Scheme
参考文献
Jasch, Hannelore; Landais, Yannick; Heinrich, Markus R.
Chemistry - A European Journal, 2013 , vol. 19, # 26 p. 8411 - 8416