反应条件
1.1: N-methyl-2-(methylamino)ethylamine; copper(l) iodide; potassium phosphate / N,N-dimethyl-formamide / 72 h / 110 °C / |Inert atmosphere 2.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium; ZnCl2*TMEDA / tetrahydrofuran; hexane / 2 h / 0 - 20 °C / |Inert atmosphere 2.2: |Inert atmosphere View Scheme
参考文献
Nagaradja, Elisabeth; Chevallier, Floris; Roisnel, Thierry; Dorcet, Vincent; Halauko, Yury S.; Ivashkevich, Oleg A.; Matulis, Vadim E.; Mongin, Florence
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 9 p. 1475 - 1487