[双(三氟乙酰氧基)碘]苯合成路线 （共 95 条）
反应条件
1: 97 percent / (CH3)3COK / CH2Cl2 / 1 h / Ambient temperature 2: 87 percent / CHCl3 / 1 h / Heating View Scheme
参考文献
Gallos, John; Varvoglis, Anastasios; Alcock, Nathaniel W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 757 - 764
反应条件
in dichloromethane 17 h; Ambient temperature;
参考文献
Boyer, Joseph H.; Natesh, Anbazhagan
Synthesis, 1988 , # 12 p. 980 - 981
反应条件
in dichloromethane
1 h; Ambient temperature;
参考文献
Macdonald, Timothy L.; Narasimhan, Narayanan
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 5000 - 5001
反应条件
in tetrachloromethane
T=0°C; 24 h; other dialkyl and aryl alkyl sulphides; other products, other solvent, different sulphide/oxidizer ratio, other time; Product distributionMechanism;
参考文献
Barbas, Dimitris; Spyroudis, Spyros; Varvoglis, Anastasios
Journal of Chemical Research, Miniprint, 1985 , # 6 p. 2201 - 2214
反应条件
iodine; magnesium; anhydrous trichlorobenzene in tetrachloromethane
参考文献
Sterling Winthrop Inc.
Patent: US5385721 A1, 1995 ;
反应条件
in chloroform
Ambient temperature; Further byproducts given;
参考文献
Gallos, John; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1999 - 2002
反应条件
water in acetonitrile
T=20°C; 24 h;
参考文献
Troian-Gautier, Ludovic; De Winter, Julien; Gerbaux, Pascal; Moucheron, Cecile
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 11096 - 11101
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-25°C; 2 h; Inert atmosphere;
参考文献
Khatri, Hem Raj; Zhu, Jianglong
Chemistry - A European Journal, 2012 , vol. 18, # 39 p. 12232 - 12236
反应条件
in chloroform
480 h;
参考文献
Gallos, John; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1999 - 2002
反应条件
iodine; sodium thiosulfate in tetrachloromethane; dichloromethane
参考文献
BioChem Pharma Inc.
Patent: US6274620 B1, 2001 ;
