N-(3-甲氧基苯基)甲酰胺合成路线 (共 16 条)
反应条件
ZnO in water T=70°C; 0.1 h; Green chemistry; chemoselective reaction;
参考文献
Alinezhad, Heshmatollah; Salehian, Fatemeh
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013 , vol. 43, # 5 p. 532 - 538
反应条件
tris-(2-chloro-ethyl)-amine; sulfuric acid in chloroform T=0°C; 0.0833333 h; Further byproducts given;
参考文献
Sprecher, Milon; Kost, Daniel
Journal of the American Chemical Society, 1994 , vol. 116, # 3 p. 1016 - 1026
反应条件
tris-(2-chloro-ethyl)-amine; sulfuric acid in chloroform T=0°C; 0.0833333 h; Further byproducts given;
参考文献
Sprecher, Milon; Kost, Daniel
Journal of the American Chemical Society, 1994 , vol. 116, # 3 p. 1016 - 1026
反应条件
1: 99 percent / 5 h / 20 °C 2: 94 percent / 2-methyl-propan-2-ol; H2O / 144 h / 20 °C View Scheme
参考文献
Vincent, Stephane; Mioskowski, Charles; Lebeau, Luc
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 991 - 997
反应条件
in tetrahydrofuran T=20°C;
参考文献
Kamijo; Jin; Yamamoto
Journal of the American Chemical Society, 2001 , vol. 123, # 38 p. 9453 - 9454
反应条件
Cu(OAc)2*2H2O; potassium carbonate T=20°C; Chan-Lam Coupling; 8 h;
参考文献
Srivastava, Vishnu P.; Yadav, Deepak K.; Yadav, Arvind K.; Watal, Geeta; Yadav, Lal Dhar S.
Synlett, 2013 , vol. 24, # 11 art. no. ST-2013-D0250-L, p. 1423 - 1427
反应条件
Lithium enolate of the acetaldehyde in tetrahydrofuran 24 h; Heating;
参考文献
Nunno, L. Di; Scilimati, A.
Tetrahedron, 1986 , vol. 42, # 14 p. 3913 - 3920
反应条件
n-butyllithium in tetrahydrofuran 1.5 h; Ambient temperature;
参考文献
Nunno, L. Di; Scilimati, A.
Tetrahedron, 1986 , vol. 42, # 14 p. 3913 - 3920
反应条件
1: 1.) n-BuLi / 1.) THF, room temp., 16 h; 2.) THF, 15 deg C, 3.5 h 2: 89 percent / n-BuLi / tetrahydrofuran / 1.5 h / Ambient temperature View Scheme
参考文献
Nunno, L. Di; Scilimati, A.
Tetrahedron, 1986 , vol. 42, # 14 p. 3913 - 3920
反应条件
in water 48 h; Reflux;
参考文献
Kaboudin, Babak; Khodamorady, Minoo
Synlett, 2010 , # 19 p. 2905 - 2907