3-氨基-5-苯基-1,2,4-噻二唑合成路线 (共 21 条)
反应条件
1: With lithium hexamethyldisilazane in tetrahydrofuran 1 h; 2: With water in tetrahydrofuran 3 h;
参考文献
Wehn, Paul M.; Harrington, Paul E.; Eksterowicz, John E.
Organic Letters, 2009 , vol. 11, # 24 p. 5666 - 5669
反应条件
An2TeO in ethanol 1 h; Ambient temperature;
参考文献
Newton, Christopher G.; Ollis, W. David; Wright, Derek E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 75 - 84
反应条件
1: 45 percent / Lawesson reagent / toluene / 0.5 h / Heating 2: PCl5 / CHCl3 / 3 h / Ambient temperature View Scheme
参考文献
Buscemi, Silvestre; Vivona, Nicolo
Heterocycles, 1994 , vol. 38, # 11 p. 2423 - 2432
反应条件
phosphorus pentachloride in chloroform 3 h; Ambient temperature;
参考文献
Buscemi, Silvestre; Vivona, Nicolo
Heterocycles, 1994 , vol. 38, # 11 p. 2423 - 2432
反应条件
1: H2S / aq. ethanol 2: H2O2 View Scheme
参考文献
Newton, Christopher G.; Ollis, W. David; Wright, Derek E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 75 - 84
反应条件
ethanol; dihydrogen peroxide
参考文献
Kurzer
Journal of the Chemical Society, 1956 , p. 4524,4527
参考文献
Butler, Richard N.; O'Donoghue, Denis A.; O'Halloran, Gerard A.
Journal of the Chemical Society, Chemical Communications, 1986 , # 10 p. 800 - 801
反应条件
ethanol anschliessend Behandeln mit Brom und Na2CO3 in Methanol;
参考文献
Goerdeler; Fincke
Chemische Berichte, 1956 , vol. 89, p. 1033,1036
反应条件
(i) K2S5, P2S5, Py, (ii) aq. H2O2; Multistep reaction;
参考文献
Goerdeler,J.; Mertens,P.
Chemische Berichte, 1970 , vol. 103, p. 1805 - 1814
反应条件
(i) NaH, THF, (ii) Br2, CHCl3, EtOH, AcOH, (iii) aq. Na2CO3; Multistep reaction;
参考文献
Junge,B.
Justus Liebigs Annalen der Chemie, 1975 , p. 1961 - 1966