1-(二氯甲基)-3-甲基苯合成路线 (共 4 条)
反应条件
tetrachloromethane; nickel; copper in N,N-dimethyl-formamide T=60°C; Chlorination; 5 h;
参考文献
Leonel, Eric; Paugam, Jean-Paul; Heintz, Monique; Nedelec, Jean-Yves
Synthetic Communications, 1999 , vol. 29, # 22 p. 4015 - 4024
反应条件
1: SnCl2; HCl; diethyl ether 2: PCl5 View Scheme
参考文献
Asinger; Lock
Monatshefte fuer Chemie, 1933 , vol. 62, p. 323,338
反应条件
2,2'-azo-bisisobutyronitrile; chlorine T=70°C; 1.2 h; various educt-reagent ratio, various time; Product distribution;
参考文献
Kosheleva, L. M.; Rozenberg, V. R.; Motsarev, G. V.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1607 - 1610
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 9 p. 1890 - 1893
参考文献
Chemical Communications, , # 13 p. 1163 - 1164