噻吩[2,3-C]并吡啶合成路线 (共 18 条)
反应条件
titanium tetrachloride in dichloromethane 24 h; Heating;
参考文献
Graulich, Amaury; Liegeois, Jean-Francois
Synthesis, 2004 , # 12 p. 1935 - 1937
反应条件
1.1: tetrahydrofuran / 0.08 h / -10 °C 1.2: tetrahydrofuran / 20 h / 20 °C 2.1: titanium tetrachloride / CH2Cl2 / 24 h / Heating View Scheme
参考文献
Nerenz, Heiko; Grahn, Walter; Jones, Peter G.
Acta Crystallographica Section C: Crystal Structure Communications, 1997 , vol. 53, # 6 p. 787 - 789
反应条件
hydrogenchloride in 1,4-dioxane
参考文献
Nerenz, Heiko; Grahn, Walter; Jones, Peter G.
Acta Crystallographica Section C: Crystal Structure Communications, 1997 , vol. 53, # 6 p. 787 - 789
反应条件
1.1: toluene / 3 h / Heating 2.1: tetrahydrofuran / 0.08 h / -10 °C 2.2: tetrahydrofuran / 20 h / 20 °C 3.1: titanium tetrachloride / CH2Cl2 / 24 h / Heating View Scheme
参考文献
Nerenz, Heiko; Grahn, Walter; Jones, Peter G.
Acta Crystallographica Section C: Crystal Structure Communications, 1997 , vol. 53, # 6 p. 787 - 789
反应条件
copper in quinoline T=205°C; 1 h;
参考文献
Farnier,M. et al.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 1066 - 1073
反应条件
pyridine; CuO/Cr2O3; coal catalyst T=425°C;
参考文献
Hansch et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1924
参考文献
Dressler,M.L.; Joullie,M.M.
Journal of Heterocyclic Chemistry, 1970 , vol. 7, p. 1257 - 1268
反应条件
1: 82 percent / K2CO3 / ethanol / 12 h / Ambient temperature; reactions of N-aminopyridinium salts 2: 5 percent / Irradiation; photolysis of thieno-, furo- and pyrrolo-<c>pyridine N-imides View Scheme
参考文献
Tsuchiya; Sawanishi; Enkaku; Hirai
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1539 - 1547
反应条件
1: 98 percent 2: 58 percent / concd. HCl / dioxane View Scheme
参考文献
Nerenz, Heiko; Grahn, Walter; Jones, Peter G.
Acta Crystallographica Section C: Crystal Structure Communications, 1997 , vol. 53, # 6 p. 787 - 789
反应条件
1: aq. KOH / 4 h / Heating 2: Cu / quinoline / 1 h / 205 °C View Scheme
参考文献
Farnier,M. et al.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 1066 - 1073