5,6-二氮杂双环[2.2.1]庚-5-烯合成路线 (共 19 条)
反应条件
oxygen in chloroform-d1 T=45°C; oxidation in several minutes in other solvents, too; Rate constant;
参考文献
Wang; Sheridan
Tetrahedron Letters, 1993 , vol. 34, # 36 p. 5673 - 5676
反应条件
T=126.9°C; other temp.; Mechanism;
参考文献
Herman, Michael S.; Goodman, Joshua L.
Journal of the American Chemical Society, 1988 , vol. 110, # 8 p. 2681 - 2683
反应条件
benzophenone; nitroxide 2 in acetonitrile Ambient temperatureIrradiation;
参考文献
Adam, Waldemar; Bottle, Steven E.
Tetrahedron Letters, 1991 , vol. 32, # 11 p. 1405 - 1408
反应条件
benzophenone in acetonitrile Ambient temperatureIrradiation;
参考文献
Adam, Waldemar; Bottle, Steven E.; Finzel, Ralf; Kammel, Thomas; Peters, Eva-Maria; et al.
Journal of Organic Chemistry, 1992 , vol. 57, # 3 p. 982 - 988
反应条件
tri-pyridin-2-yl-[1,3,5]triazine in dichloromethane Irradiation; Product distribution;
参考文献
Koner, Apurba L.; Marquez, Cesar; Dickman, Michael H.; Nau, Werner M.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 2 p. 545 - 548
反应条件
in n-heptane T=25°C; 0.166667 h; Irradiationother solvent, other temperature; Product distribution;
参考文献
Adam, Waldemar; Oppenlaender, Thomas
Tetrahedron Letters, 1982 , vol. 23, # 51 p. 5391 - 5394
反应条件
1-(4-methoxyphenyl)ethanone in acetonitrile-D3 Elimination; cyclization; Photolysis; Kinetics;
参考文献
Showalter, Brett M.; Bentz, Timothy C.; Ryzhkov, Lev R.; Hadad, Christopher M.; Toscano, John P.
Journal of Physical Organic Chemistry, 2000 , vol. 13, # 6 p. 309 - 312
反应条件
oxygen; benzophenone in n-heptane T=8°C; P=760 - 7600 Torr; Irradiationeffect of solvents; Rate constant;
参考文献
Adam, Waldemar; Hoessel, Peter; Huemmer, Walter; Platsch, Herbert
Journal of the American Chemical Society, 1987 , vol. 109, # 24 p. 7570 - 7572
反应条件
oxygen; 1-(4-methoxyphenyl)ethanone in acetonitrile-D3 Elimination; oxidation; Photolysis; Kinetics;
参考文献
Showalter, Brett M.; Bentz, Timothy C.; Ryzhkov, Lev R.; Hadad, Christopher M.; Toscano, John P.
Journal of Physical Organic Chemistry, 2000 , vol. 13, # 6 p. 309 - 312
反应条件
benzophenone; cyclohexene in benzene Ambient temperatureIrradiationfurther solvent: n-heptane; Product distributionMechanism;
参考文献
Adam, Waldemar; Finzel, Ralf; Walther, Barbara
Chemische Berichte, 1993 , vol. 126, # 9 p. 2137 - 2142