反应条件
1: pyridinium chlorochromate (PCC) / CH2Cl2
2: 1.) n-BuLi / 1.) THF, hexane, DMSO, RT, 30 min, 2.) THF, hexane, DMSO, RT, 3 h
3: 98 percent / H2 / PtO2 / methanol / Ambient temperature
View Scheme
参考文献
Carballeira, Nestor; Thompson, Janice E.; Ayanoglu, Eser; Djerassi, Carl
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2751 - 2756
