5-叔丁基-2-羟基苯甲醛合成路线 （共 22 条）
反应条件
triethylamine; magnesium chloride in acetonitrile 3 h; Heating;
参考文献
Knight, Paul D.; O'Shaughnessy, Paul N.; Munslow, Ian J.; Kimberley, Brian S.; Scott, Peter
Journal of Organometallic Chemistry, 2003 , vol. 683, # 1 p. 103 - 113
反应条件
sodium hydroxide in methanol; water T=65°C; 2 h;
参考文献
Stepniak-Biniakiewicz, Danuta
Polish Journal of Chemistry, 1980 , vol. 54, # 7/8 p. 1567 - 1571
反应条件
trifluoroacetic acid 1.5 h; Heating;
参考文献
Lindoy, Leonard F.; Meehan, George V.; Svenstrup, Niels
Synthesis, 1998 , # 7 p. 1029 - 1032
反应条件
chloroform; potassium hydroxide in water T=60°C; Reimer-Tiemann Phenol Formylation; 15 h;
参考文献
Zhang, Shuai; Wan, Changfeng; Wang, Qiang; Zhang, Baiqun; Gao, Lingfeng; Zha, Zhenggen; Wang, Zhiyong
European Journal of Organic Chemistry, 2013 , # 11 p. 2080 - 2083
反应条件
1: 4-tert-butyl-phenol With magnesium methanolate in methanol; toluene 1 h; Heating; 2: (CH2O)x in toluene T=110°C; 3 h; 3: With sulfuric acid in toluene T=60°C; 1.5 h;
参考文献
Singer, Robert A.; Brock, Jane R.; Carreira, Erick M.
Helvetica Chimica Acta, 2003 , vol. 86, # 4 p. 1040 - 1044
反应条件
triethylamine; magnesium chloride in tetrahydrofuran 5 h; Inert atmosphereReflux;
参考文献
Biannic, Berenger; Bozell, Joseph J.
Organic Letters, 2013 , vol. 15, # 11 p. 2730 - 2733
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in acetic acid 4 h; Heating;
参考文献
Stokker, G. E.; Schultz, E. M.
Synthetic Communications, 1982 , vol. 12, # 11 p. 847 - 854
反应条件
in methanol; toluene 3 h; Heating;
参考文献
Plieger, Paul G.; Tasker, Peter A.; Galbraith, Stuart G.
Dalton Transactions, 2004 , # 2 p. 313 - 318
反应条件
1: zinc chloride / 180 °C 2: NaOH; water View Scheme
参考文献
Dains; Rothrock
American Chemical Journal, 1894 , vol. 16, p. 635
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 20 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 32 p. 11509 - 11518
