5-叔丁基-2-羟基苯甲醛合成路线 （共 22 条）
反应条件
1: 5-(1,1-dimethylethyl)salicylaldehyde With nitronium tetrafluoroborate in acetonitrile
T=-40 - -20°C; 1 h;
2: methyl iodide With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 15 h;
参考文献
TORAY INDUSTRIES, INC.
Patent: US2012/184735 A1, 2012 ;
Location in patent: Page/Page column 17 ;
反应条件
1: nitric acid / acetic acid / 2 h / 20 °C
2: potassium carbonate / toluene / 4 h / Reflux
View Scheme
参考文献
Guieu, Samuel; Crane, Angela K.; MacLachlan, Mark J.
Chemical Communications, 2011 , vol. 47, # 4 p. 1169 - 1171
