2,4-环戊二烯-1-基(三甲基)锡烷合成路线 （共 13 条）
反应条件
in tetrahydrofuran 3 h, reflux;;
参考文献
Angewandte Chemie, , vol. 83, p. 360 - 361
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1706 - 1711
反应条件
in tetrahydrofuran 2 h, reflux;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1.9, page 93 - 108
反应条件
in dimethyl sulfoxide; benzene Kinetics; in presence of I(1-);;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 9, p. 2231 - 2239
Zhurnal Organicheskoi Khimii, , vol. 9, p. 2215 - 2223
反应条件
in ethylene glycol dimethyl ether boiling DME;
参考文献
Journal of Organometallic Chemistry, , vol. 22, p. C31 - C32
反应条件
in diethyl ether Ar atmosphere or vac.; addn. of InCl to soln. of Me3SnC5H5 (room temp., darkness, stirring, 12 h); removal of solvent (distn, vac, -20°C), removal of Me3SnCl (sublimation), sublimation (80°C);
参考文献
Organometallics, , vol. 9, p. 2488 - 2492
反应条件
mercury dichloride Kinetics;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 9, p. 1119 - 1126
Zhurnal Organicheskoi Khimii, , vol. 9, p. 1089 - 1098
参考文献
Gmelin Handbook: Co: Org.Verb.1, 1.1.4.5.2.10.1, page 141 - 144
反应条件
mercury dichloride Kinetics;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1.9, page 93 - 108
反应条件
in toluene Ce(O-i-Pr)4 is dissolved in toluene, soln. of Me3SnCp is added, mixt. is heated at 65°C for 24 h (N2); mixt. is ccoled to room temp., filtn., volatile components are removed under high vac., recrystn. at -78°C (pentane) or sublimation at 70°C (10E-5 Torr); elem. anal.;
参考文献
Gulino, Antonio; Casarin, Maurizio; Conticello, Vincent P.; Gaudiello, John G.; Mauermann, Heiko; et al.
Organometallics, 1988 , vol. 7, p. 2360 - 2364
反应条件
in tetrahydrofuran 20 °C;;
参考文献
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1.9, page 93 - 108
