1: 4-Amino-5-chloro-2-methoxy benzoic acid With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-[1,3,5]triazine in N,N-dimethyl-formamide T=20°C; 1 h; 2: N-[2-(ethylamino)ethyl]amine in N,N-dimethyl-formamide T=20°C; 19 h;

1: m-chloroperbenzoic acid / CH2Cl2 / 0.33 h / Ambient temperature 2: aq. FeCl2 / CH2Cl2 / Ambient temperature View Scheme

iron(II) chloride in dichloromethane Ambient temperature; Yield given;