N,N-二乙基-4-甲基苯甲酰胺合成路线 （共 21 条）
反应条件
tert.-butylhydroperoxide; Cu(ClO4)2*6H2O T=100°C; 15 h;
参考文献
Kumar, P. Santhosh; Kumar, G. Sathish; Kumar, R. Arun; Reddy, N. Veera; Rajender Reddy
European Journal of Organic Chemistry, 2013 , # 7 p. 1218 - 1222
反应条件
in tetrahydrofuran T=20°C; 4 h;
参考文献
Katritzky; He; Suzuki
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8210 - 8213
反应条件
1: With palladium diacetate T=20°C; 0.166667 h; Inert atmosphere; 2: With trichlorophosphate T=140°C; 5 h; Inert atmosphere;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Motevalli, Somayeh
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 355, p. 69 - 74
反应条件
1: Iron (III) nitrate nonahydrate; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical / acetonitrile / 2 h / 20 °C / |Inert atmosphere; |Green chemistry 2: tert.-butylhydroperoxide; calcium carbonate / water / 16 h / 60 °C / |Inert atmosphere; |Green chemistry View Scheme
参考文献
Ghosh, Subhash Chandra; Ngiam, Joyce S.Y.; Seayad, Abdul M.; Tuan, Dang Thanh; Johannes, Charles W.; Chen, Anqi
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4922 - 4925
反应条件
in acetonitrile 2 h; Ambient temperature; Yield given;
参考文献
Kikukawa, Kiyoshi; Kono, Kiyoshi; Nagira, Kazuhiko; Wada, Fumio; Matsuda, Tsutomu
Journal of Organic Chemistry, 1981 , vol. 46, p. 4413 - 4416
反应条件
tetrachlorosilane; benzene Behandeln des von SiCl4 befreiten Reaktionsgemisches mit Diaethylamin;
参考文献
Jur'ew et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2594,2595, 2596; engl. Ausg. S. 2557, 2558
反应条件
lanthanum trifluoromethanesulphonate 1.) THF, -78 deg C then up to 0 deg C, 2.) -78 deg C, 20 min; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 55, # 11 p. 3565 - 3568
反应条件
sodium in tetrahydrofuran 5 h; Ambient temperatureultrasonic bath; also Li as reagent;
参考文献
Tetrahedron Letters, , vol. 31, # 7 p. 941 - 944
反应条件
1.1: sec-BuLi; TMEDA / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C 1.2: 71 percent / tetrahydrofuran; cyclohexane / -78 - 20 °C 2.1: 77 percent / LDA / tetrahydrofuran / -78 - 20 °C 3.1: 92 percent / NaBH4; NaOH / methanol; H2O / 13 h / Heating View Scheme
参考文献
Mukherjee, Chandrani; Kamila, Sukanta; De, Asish
Tetrahedron, 2003 , vol. 59, # 26 p. 4767 - 4774
反应条件
sodium in tetrahydrofuran 5 h; Ambient temperatureultrasonic bath; also Li as reagent;
参考文献
Tetrahedron Letters, , vol. 31, # 7 p. 941 - 944
