(S)-1-(4-甲基苯基)乙胺合成路线 （共 18 条）
反应条件
1: ethanol; sodium 2: (1R)-cis-camphoric acid View Scheme
参考文献
Ingersoll; Burns
Journal of the American Chemical Society, 1932 , vol. 54, p. 4712,4714
反应条件
1: toluene; diethyl ether / 0.42 h / -20 °C 2: 72 percent / Mo(CO)6 / acetonitrile; H2O / 1 h / 85 °C View Scheme
参考文献
Atobe, Masakazu; Yamazaki, Naoki; Kibayashi, Chihiro
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5595 - 5607
反应条件
1: 98 percent / TsOH / toluene / 0.5 h / Heating 2: toluene; diethyl ether / 0.42 h / -20 °C 3: 72 percent / Mo(CO)6 / acetonitrile; H2O / 1 h / 85 °C View Scheme
参考文献
Atobe, Masakazu; Yamazaki, Naoki; Kibayashi, Chihiro
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5595 - 5607
反应条件
Chromobacterium violaceum ω-transaminase variant W60C T=37°C; pH=7; 12 h; Reagent/catalystpH-value; enantioselective reaction;
参考文献
Wang, Bo; Land, Henrik; Berglund, Per
Chemical Communications, 2013 , vol. 49, # 2 p. 161 - 163
反应条件
Ni T=110°C; 2 h; Inert atmosphere;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
反应条件
hydrogen; Pd-BaSO4 in toluene T=70°C; P=75.0075 Torr; 24 h; Kinetics;
参考文献
Parvulescu, Andrei N.; Jacobs, Pierre A.; De Vos, Dirk E.
Chemistry - A European Journal, 2007 , vol. 13, # 7 p. 2034 - 2043
反应条件
Ni T=110°C; 2 h; Inert atmosphere;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
反应条件
hydrogen; Pd-BaSO4 in toluene T=70°C; P=75.0075 Torr; 24 h; Kinetics;
参考文献
Parvulescu, Andrei N.; Jacobs, Pierre A.; De Vos, Dirk E.
Chemistry - A European Journal, 2007 , vol. 13, # 7 p. 2034 - 2043
