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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并恶唑
合成路线
（共 384 条）
273-53-0
苯并恶唑
+
1666-17-7
苯甲醛对甲苯磺酰腙
→
反应条件
2008-07-3
2-(苯基甲基)-1,3-苯并恶唑
反应条件
copper(l) iodide; lithium tert-butylate in 1,4-dioxane T=120°C; 1.5 h; Inert atmosphere;
参考文献
Zhao, Xia; Wu, Guojiao; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 10 p. 3296 - 3299
273-53-0
苯并恶唑
+
100-44-7
苄基氯
→
反应条件
2008-07-3
2-(苯基甲基)-1,3-苯并恶唑
反应条件
potassium phosphate; 1,3-bis-(diphenylphosphino)propane; palladium diacetate in N,N-dimethyl-formamide T=120°C; 16 h; chemoselective reaction;
参考文献
Xie, Pan; Huang, Hanmin; Xie, Yinjun; Guo, Shengmei; Xia, Chungu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1692 - 1700
273-53-0
苯并恶唑
+
100-44-7
苄基氯
→
反应条件
2008-07-3
2-(苯基甲基)-1,3-苯并恶唑
反应条件
potassium phosphate; palladium (II) trifluoroacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide T=120°C; 16 h; Inert atmosphere; chemoselective reaction;
参考文献
Xie, Pan; Huang, Hanmin; Xie, Yinjun; Guo, Shengmei; Xia, Chungu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1692 - 1700
273-53-0
苯并恶唑
+
99-90-1
4-溴苯乙酮
→
反应条件
37069-08-2
反应条件
PdCl(C3H5)(dppb); caesium carbonate in carbonic acid diethyl ester T=130°C; 17 h; Inert atmosphere; regioselective reaction;
参考文献
Dong, Jia Jia; Roger, Julien; Verrier, Cecile; Martin, Thibaut; Le Goff, Ronan; Hoarau, Christophe; Doucet, Henri
Green Chemistry, 2010 , vol. 12, # 11 p. 2053 - 2063
273-53-0
苯并恶唑
+
99-91-2
对氯苯乙酮
→
反应条件
37069-08-2
反应条件
caesium carbonate; PdCl(C3H5)(dppb) in N,N-dimethyl-formamide T=120°C; 20 h;
参考文献
Derridj, Fazia; Djebbar, Safia; Benali-Baitich, Ouassini; Doucet, Henri
Journal of Organometallic Chemistry, 2008 , vol. 693, # 1 p. 135 - 144
273-53-0
苯并恶唑
+
13329-40-3
4-碘代苯乙酮
→
反应条件
37069-08-2
反应条件
potassium phosphate; Cu2(4,4’-biphenyldicarboxylate)2(4,4’-bipyridine) in α-n-hexadecene; N,N-dimethyl-formamide T=120°C; 3 h; Green chemistry;
参考文献
Le, Hanh T.N.; Nguyen, Tung T.; Vu, Phuong H.L.; Truong, Thanh; Phan, Nam T.S.
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 391, # 1 p. 74 - 82
273-53-0
苯并恶唑
+
1788-10-9
4-乙酰基苯磺酰氯
→
反应条件
37069-08-2
反应条件
copper(l) iodide; oxygen; palladium diacetate; potassium carbonate in 1,4-dioxane T=120°C; 48 h; Sealed tube;
参考文献
Zhang, Manli; Zhang, Shouhui; Liu, Miaochang; Cheng, Jiang
Chemical Communications, 2011 , vol. 47, # 41 p. 11522 - 11524
273-53-0
苯并恶唑
+
40307-11-7
4-乙基苯乙炔
→
反应条件
37135-35-6
2-(4-乙基苯基)-苯并噁唑
反应条件
oxygen; caesium carbonate; silver carbonate; bis(dibenzylideneacetone)-palladium(0) in dimethyl sulfoxide; N,N-dimethyl-formamide T=140°C; 11 h;
参考文献
Liu, Dongfang; Liu, Bin; Cheng, Jiang
RSC Advances, 2013 , vol. 3, # 24 p. 9193 - 9196
273-53-0
苯并恶唑
+
4748-78-1
4-乙基苯甲醛
→
反应条件
37135-35-6
2-(4-乙基苯基)-苯并噁唑
反应条件
iodine; N,N-dimethyl-formamide in chlorobenzene T=130°C;
参考文献
Teo, Yew Chin; Riduan, Siti Nurhanna; Zhang, Yugen
Green Chemistry, 2013 , vol. 15, # 9 p. 2365 - 2368
273-53-0
苯并恶唑
+
63139-21-9
4-乙基苯硼酸
→
反应条件
37135-35-6
2-(4-乙基苯基)-苯并噁唑
反应条件
[2,2']bipyridinyl; potassium phosphate; Ni2(BDC)2(1,4-diazabicyclo[2.2.2]octane) in N,N-dimethyl acetamide T=100°C; 3 h;
参考文献
Phan, Nam T. S.; Nguyen, Chung K.; Nguyen, Tung T.; Truong, Thanh
Catalysis Science and Technology, 2014 , vol. 4, # 2 p. 369 - 377
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