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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并恶唑
合成路线
(共 384 条)
273-53-0
苯并恶唑
+
335343-05-0
→
反应条件
13459-17-1
反应条件
oxygen; copper(l) chloride; lithium tert-butylate in N,N-dimethyl-formamide T=40°C; P=760.051 Torr; 0.166667 h;
参考文献
Yang, Fanzhi; Xu, Zhaoqing; Wang, Zhe; Yu, Zhengkun; Wang, Rui
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6321 - 6325
273-53-0
苯并恶唑
+
529-28-2
2-碘苯甲醚
→
反应条件
13459-17-1
反应条件
potassium carbonate; copper(II) oxide in diethylene glycol dimethyl ether 3 h; Inert atmosphereReflux;
参考文献
Zhang, Wu; Zeng, Qinglong; Zhang, Xinming; Tian, Yujie; Yue, Yun; Guo, Yujun; Wang, Zhenghua
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4741 - 4745
273-53-0
苯并恶唑
+
15898-38-1
→
反应条件
14625-58-2
反应条件
1: With copper diacetate; palladium diacetate; trifluoroacetic acid in ethylene glycol dimethyl ether T=120°C; 24 h; Inert atmosphereSealed tube; 2: With potassium carbonate in ethylene glycol dimethyl ether; water T=20°C;
参考文献
Wang, Min; Li, Dengke; Zhou, Wei; Wang, Lei
Tetrahedron, 2012 , vol. 68, # 7 p. 1926 - 1930
273-53-0
苯并恶唑
+
19169-97-2
→
反应条件
14625-58-2
反应条件
1,10-phenanthroline; palladium diacetate; caesium carbonate in dimethyl sulfoxide T=150°C; 20 h; Inert atmosphere;
参考文献
Yu, Peng; Zhang, Guangyou; Chen, Fan; Cheng, Jiang
Tetrahedron Letters, 2012 , vol. 53, # 34 p. 4588 - 4590
273-53-0
苯并恶唑
+
17933-03-8
3-甲基苯硼酸
→
反应条件
14625-58-2
反应条件
anhydrous iron chloride; Cu(OAc)2*2H2O; palladium dichloride in N,N-dimethyl-formamide T=120°C; 24 h;
参考文献
Wu, Xiang-Mei; Shen, Qiu-Xian
Letters in Organic Chemistry, 2013 , vol. 10, # 9 p. 668 - 673
273-53-0
苯并恶唑
+
3955-72-4
→
反应条件
14625-58-2
反应条件
palladium diacetate; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide; tert-butyl alcohol T=100°C; 21 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Althammer, Andreas; Fenner, Sabine
Angewandte Chemie - International Edition, 2009 , vol. 48, # 1 p. 201 - 204
273-53-0
苯并恶唑
+
223799-24-4
→
反应条件
14625-58-2
反应条件
oxygen; copper(l) chloride; lithium tert-butylate in N,N-dimethyl-formamide T=40°C; P=760.051 Torr; 0.166667 h;
参考文献
Yang, Fanzhi; Xu, Zhaoqing; Wang, Zhe; Yu, Zhengkun; Wang, Rui
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6321 - 6325
273-53-0
苯并恶唑
+
55510-25-3
→
反应条件
14625-58-2
反应条件
dichloro bis(acetonitrile) palladium(II); 1,10-phenanthroline; tetrabutylammomium bromide; copper diacetate; sodium carbonate in 1,4-dioxane; dimethyl sulfoxide T=20 - 100°C; 4.58333 h; Inert atmosphere;
参考文献
Yu, Xinzhang; Li, Xingwei; Wan, Boshun
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 37 p. 7479 - 7482
273-53-0
苯并恶唑
+
108-41-8
→
反应条件
14625-58-2
反应条件
PdCl2(C3H3N2(CH3))(C3H2N2(C6H3(C3H7)2)2); lithium tert-butylate in toluene T=130°C; 18 h; Inert atmosphere;
参考文献
Shen, Xiao-Bao; Zhang, Yun; Chen, Wen-Xin; Xiao, Zheng-Kang; Hu, Ting-Ting; Shao, Li-Xiong
Organic Letters, 2014 , vol. 16, # 7 p. 1984 - 1987
273-53-0
苯并恶唑
+
32578-31-7
→
反应条件
14625-58-2
反应条件
[Ni0(1,5-cyclooctadiene)2]; caesium carbonate; dcype in 1,4-dioxane T=120°C; 12 h; Inert atmosphere;
参考文献
Muto, Kei; Yamaguchi, Junichiro; Itami, Kenichiro
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 169 - 172
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