2-(甲基磺酰基)-1-(2-吡啶基)-乙酮合成路线 （共 6 条）
反应条件
triethylamine in dichloromethane 1.) ice cooling, 1 h; 2.) R.T., 2 h; than overnight.;
参考文献
Koikov, L. N.; Terent'ev, P. B.; Gloriozov, I. P.; Torocheshnikov, V. N.; Baidin, V. N.; Bundel', Yu. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 5 p. 518 - 524
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 5 p. 643 - 650
反应条件
1: 97.5 percent / methanol / Ambient temperature 2: 93 percent / sodium metaperiodate / further reagent 3: m-cloroperbenzoic acid View Scheme
参考文献
Ruano, J. L. Garcia; Pedregal, C.; Rodriguez, J. H.
Tetrahedron, 1987 , vol. 43, # 19 p. 4407 - 4416
反应条件
1: 18.9 percent / bromine / benzene; acetic acid / 60 °C 2: 97.5 percent / methanol / Ambient temperature 3: 93 percent / sodium metaperiodate / further reagent 4: m-cloroperbenzoic acid View Scheme
参考文献
Ruano, J. L. Garcia; Pedregal, C.; Rodriguez, J. H.
Tetrahedron, 1987 , vol. 43, # 19 p. 4407 - 4416
反应条件
1: 20 percent / TiCl4 / benzene; diethyl ether / -15 - -5 °C 2: 0.2 percent / triethylamine / CH2Cl2 / 1.) ice cooling, 1 h; 2.) R.T., 2 h; than overnight. View Scheme
参考文献
Koikov, L. N.; Terent'ev, P. B.; Gloriozov, I. P.; Torocheshnikov, V. N.; Baidin, V. N.; Bundel', Yu. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 5 p. 518 - 524
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 5 p. 643 - 650
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Ruano, J. L. Garcia; Pedregal, C.; Rodriguez, J. H.
Tetrahedron, 1987 , vol. 43, # 19 p. 4407 - 4416
反应条件
1: 93 percent / sodium metaperiodate / further reagent 2: m-cloroperbenzoic acid View Scheme
参考文献
Ruano, J. L. Garcia; Pedregal, C.; Rodriguez, J. H.
Tetrahedron, 1987 , vol. 43, # 19 p. 4407 - 4416
