(R,s)-n-乙酰基-3,4-二甲氧基苯丙氨酸合成路线 （共 6 条）
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Oltz,E.M.; Bruening,R.C.; Smith,M.J.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6162
反应条件
1: 51 percent / water / acetone / Heating 2: 94 percent / H2 / 5 percent Pd/C / methanol View Scheme
参考文献
Oltz,E.M.; Bruening,R.C.; Smith,M.J.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6162
反应条件
1: 60 percent / acetic anhydride, NaOAc / acetic acid / 1.) 80 deg C, 10 min, 2.) 143 deg C, 1 h 2: 51 percent / water / acetone / Heating 3: 94 percent / H2 / 5 percent Pd/C / methanol View Scheme
参考文献
Oltz,E.M.; Bruening,R.C.; Smith,M.J.
Journal of the American Chemical Society, 1988 , vol. 110, p. 6162
反应条件
hydrogenchloride in water T=95 - 100°C; 6 h;
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897
反应条件
1: SOCl2 / Heating 2: (i) NaBH4, aq. EtOH, (ii) aq. HCl View Scheme
参考文献
Seki; Koga; Yamada
Chemical and pharmaceutical bulletin, 1967 , vol. 15, # 12 p. 1948 - 1954
参考文献
Tolstikov; Karpyshev; Tolstikova; Khlebnikova; Sal'nikov; Mamatyuk; Gatilov; Bagryanskaya
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 8 p. 1134 - 1148
