1,10-邻二氮杂菲-5,6-二酮合成路线 （共 33 条）
反应条件
in tetrahydrofuran 4 h; Heating;
参考文献
Van der Tol, Erik B.; Van Ramesdonk, Hendrik J.; Verhoeven, Jan W.; Steemers, Frank J.; Kerver, Esther G.; Verboom, Willem; Reinhoudt, David N.
Chemistry - A European Journal, 1998 , vol. 4, # 11 p. 2315 - 2323
反应条件
in tetrahydrofuran 4 h; Heating;
参考文献
Koninklijke Philips Electronics N.V.
Patent: EP1019401 B1, 2008 ;
Location in patent: Page/Page column 4-6 ;
反应条件
in ethanol 5 h; Inert atmosphereReflux;
参考文献
Francois, Angelica; Diaz, Ramiro; Ramirez, Angelica; Loeb, Barbara; Barrera, Mauricio; Crivelli, Irma
Polyhedron, 2013 , vol. 52, p. 62 - 71
反应条件
in ethanol; water T=180°C; 24 h;
参考文献
Che, Guangbo; Li, Wenlian; Kong, Zhiguo; Su, Zisheng; Chu, Bei; Li, Bin; Zhang, Zhiqiang; Hu, Zhizhi; Chi, Haijun
Synthetic Communications, 2006 , vol. 36, # 17 p. 2519 - 2524
参考文献
Ivanov; Puzyk; Balashev
Russian Journal of General Chemistry, 2006 , vol. 76, # 6 p. 843 - 848
反应条件
ammonium acetate; ammonia in ethanol 168 h; Reflux;
参考文献
Jayabharathi, Jayaraman; Thanikachalam, Venugopal; Venkatesh Perumal, Marimuthu; Srinivasan, Natesan
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2011 , vol. 79, # 1 p. 236 - 244
反应条件
in ethanol soln. Ru complex and ligand in EtOH was heated to reflux for 10 h under N2 atm.; solvent was removed in vacuo, chromy. on silica (CH2Cl2-MeCN); elem. anal.;
参考文献
Ghumaan, Sandeep; Sarkar, Biprajit; Patra, Srikanta; Van Slageren, Joris; Fiedler, Jan; Kaim, Wolfgang; Lahiri, Goutam Kumar
Inorganic Chemistry, 2005 , vol. 44, # 9 p. 3210 - 3214
反应条件
1: 83 percent / Na2CO3; NH2OH*HCl / ethanol / 5 h / Heating 2: 89 percent / H2 / Pd/C / ethanol / 24 h / 20 °C / 3750.3 Torr View Scheme
参考文献
Zhang, Pingyu; Wang, Jinquan; Huang, Huaiyi; Qiao, Liping; Ji, Liangnian; Chao, Hui
Dalton Transactions, 2013 , vol. 42, # 24 p. 8907 - 8917
反应条件
potassium permanganate in water Heating;
参考文献
Baxter, Paul N. W.; Connor, Joseph A.; Wallis, John D.; Povey, David C.; Powell, Anne K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1601 - 1606
反应条件
1: ethanol / 5 h / |Inert atmosphere; |Reflux
2: sulfuric acid / 5 h / |Reflux
View Scheme
参考文献
Francois, Angelica; Diaz, Ramiro; Ramirez, Angelica; Loeb, Barbara; Barrera, Mauricio; Crivelli, Irma
Polyhedron, 2013 , vol. 52, p. 62 - 71
