3,5-二苄氧基苯甲酸甲酯合成路线 （共 24 条）
反应条件
potassium hydroxide in ethanol 18 h; Heating;
参考文献
Meltzer, Peter C.; Dalzell, Haldean C.; Razdan, Raj K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2825 - 2829
反应条件
hydrogenchloride; sodium hydroxide in ethanol
参考文献
Rhone-Poulenc Rorer Pharmaceuticals Inc.
Patent: US5232948 A1, 1993 ;
US 5232948 A
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C;
参考文献
Hsu; Rice; Brossi
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1576 - 1589
反应条件
1: With sodium hydroxide in water 16 h; Reflux; 2: With hydrogenchloride in water Cooling with ice;
参考文献
Resch, Verena; Lechner, Horst; Schrittwieser, Joerg H.; Wallner, Silvia; Gruber, Karl; MacHeroux, Peter; Kroutil, Wolfgang
Chemistry - A European Journal, 2012 , vol. 18, # 41 p. 13173 - 13179
反应条件
1: 84 percent / Et3N / CH2Cl2 / 0.33 h / 4 °C 2: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 3: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C View Scheme
参考文献
Meltzer, Peter C.; Dalzell, Haldean C.; Razdan, Raj K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2825 - 2829
反应条件
1: 96 percent / K2CO3 / acetone / 12 h / Heating 2: 97 percent / LiAlH4 3: 84 percent / Et3N / CH2Cl2 / 0.33 h / 4 °C 4: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 5: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C View Scheme
参考文献
Meltzer, Peter C.; Dalzell, Haldean C.; Razdan, Raj K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2825 - 2829
反应条件
1: 97 percent / LiAlH4 2: 84 percent / Et3N / CH2Cl2 / 0.33 h / 4 °C 3: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 4: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C View Scheme
参考文献
Meltzer, Peter C.; Dalzell, Haldean C.; Razdan, Raj K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2825 - 2829
反应条件
1: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 2: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C View Scheme
参考文献
Meltzer, Peter C.; Dalzell, Haldean C.; Razdan, Raj K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2825 - 2829
反应条件
1.1: K2CO3 / dimethylformamide / 20 °C 2.1: aq. KOH / ethanol / 20 °C 3.1: SOCl2 4.1: Et3N / tetrahydrofuran / 0 °C 5.1: silver benzoate; Et3N / methanol 5.2: aq. KOH / methanol View Scheme
参考文献
Meltzer, Peter C.; Dalzell, Haldean C.; Razdan, Raj K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2825 - 2829
反应条件
1.1: SOCl2 2.1: Et3N / tetrahydrofuran / 0 °C 3.1: silver benzoate; Et3N / methanol 3.2: aq. KOH / methanol View Scheme
参考文献
Hill, Robert A.; Carter, Rachel H.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2570 - 2576
