(9Z)-11-[(2S,3R)-3-戊基-2-环氧乙烷基]-9-十一碳烯酸甲酯合成路线 (共 5 条)
反应条件
1.1: sodium methylate / methanol / 2 h / Reflux 1.2: 24.25 h / 0 °C 2.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / Reflux View Scheme
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
1: With sodium methylate in methanol 2 h; Reflux; 2: in methanol T=0°C; 24.25 h;
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
1: With sodium methylate in methanol 2 h; Reflux; 2: in methanol T=0°C; 24.25 h;
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
1: With sodium methylate in methanol 2 h; Reflux; 2: in methanol T=0°C; 24.25 h;
参考文献
Johnson, Nikki S.; Ayorinde, Folahan O.
JAOCS, Journal of the American Oil Chemists' Society, 2011 , vol. 88, # 9 p. 1425 - 1430
反应条件
1: With sodium hydroxide in tetrahydrofuran; water
T=23°C; 6 h;
2: With hydrogenchloride in tetrahydrofuran; water
pH=4.5;
参考文献
Falck; Reddy; Haines, Donovan C.; Reddy, Komandla Malla; Krishna; Graham, Sandra; Murry, Barbara; Peterson, Julian A.
Tetrahedron Letters, 2001 , vol. 42, # 25 p. 4131 - 4133