1-(1,3,5-环庚三烯-1-基)乙酮合成路线 （共 4 条）
反应条件
1: 50 percent / AlCl3 / CH2Cl2 / 2 h / Heating 2: 66 percent / NaOH, Br2 / H2O; dioxane 3: SOCl2, pyridine / 55 °C 4: 61 percent / Lithium-tri-tert-butoxyhydridoaluminat / tetrahydrofuran / -70 °C View Scheme
参考文献
Vogel, Emanuel; Deger, Hans M.; Sombroek, Johannes; Palm, Juergen; Wagner, Arwed; Lex, Johann
Angewandte Chemie, 1980 , vol. 92, # 1 p. 43 - 45
反应条件
oxygen; 5,15,10,20-tetraphenylporphyrin in tetrachloromethane T=10°C; Irradiation;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 14 p. 2071 - 2077
反应条件
1: 56 percent / Br2, aq. NaOH / dioxane / 2.5 h / 0 - 20 °C 2: thionyl chloride, pyridine / 1 h / Heating View Scheme
参考文献
Higuchi, Hiroyuki; Kondo, Masao; Yonehara, Hiroko; Ojima, Juro; Iyoda, Masahiko
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 1 p. 275 - 281
反应条件
1: 56 percent / Br2, aq. NaOH / dioxane / 2.5 h / 0 - 20 °C
2: 89 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating
3: 64 percent / BaMnO4 / CH2Cl2 / 23 h / Ambient temperature
View Scheme
参考文献
Higuchi, Hiroyuki; Kondo, Masao; Yonehara, Hiroko; Ojima, Juro; Iyoda, Masahiko
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 1 p. 275 - 281
