1,3,3-三甲基吲哚-奈谔嗪合成路线 （共 14 条）
反应条件
sodium hydrogencarbonate; magnesium sulfate in dimethyl sulfoxide; toluene T=80°C; 12 h;
参考文献
Lokshin, Vladimir; Samat, Andre; Guglielmetti, Robert
Tetrahedron, 1997 , vol. 53, # 28 p. 9669 - 9678
反应条件
T=110°C; 0.2 h; microwave irradiation;
参考文献
Koshkin; Fedorova; Lokshin; Guglielmetti; Hamelin; Texier-Boullet; Gromov
Synthetic Communications, 2004 , vol. 34, # 2 p. 315 - 322
反应条件
1: 1-nitroso-2-hydroxy-naphthalene; 1-aza-15-crown-5 in methanol T=80°C; 6 h; 2: 1,3-dihydro-1,3,3-trimethyl-2-methyleneindoline in methanol T=80°C; 2.5 h;
参考文献
Fedorova, Olga A.; Strokach, Yuri P.; Gromov, Sergey P.; Koshkin, Alexander V.; Valova, Tatjana M.; Alfimov, Michael V.; Feofanov, Alexei V.; Alaverdian, Iouri S.; Lokshin, Vladimir A.; Samat, Andre; Guglielmetti, Robert; Girling, Reuben B.; Moore, John N.; Hester, Ronald E.
New Journal of Chemistry, 2002 , vol. 26, # 9 p. 1137 - 1145
反应条件
1: 26 percent / Et3N; DMSO / toluene / 20 h / 20 °C 2: methanol / Heating View Scheme
参考文献
Koshkin; Lokshin; Samat; Gromov; Fedorova
Synthesis, 2005 , # 11 art. no. Z21004SS, p. 1876 - 1880
反应条件
1: 26 percent / Et3N; DMSO / toluene / 20 h / 20 °C 2: methanol / Heating View Scheme
参考文献
Koshkin; Lokshin; Samat; Gromov; Fedorova
Synthesis, 2005 , # 11 art. no. Z21004SS, p. 1876 - 1880
反应条件
1: 1-aza-18-crown-6; 1-nitroso-2-hydroxy-naphthalene in methanol 2: 1,3-dihydro-1,3,3-trimethyl-2-methyleneindoline With triethylamine in methanol Further stages.;
参考文献
Fedorova, Olga A.; Strokach, Yuri P.; Gromov, Sergey P.; Koshkin, Alexander V.; Valova, Tatjana M.; Alfimov, Michael V.; Feofanov, Alexei V.; Alaverdian, Iouri S.; Lokshin, Vladimir A.; Samat, Andre; Guglielmetti, Robert; Girling, Reuben B.; Moore, John N.; Hester, Ronald E.
New Journal of Chemistry, 2002 , vol. 26, # 9 p. 1137 - 1145
反应条件
in acetonitrile-D3 T=-45.15°C; Cyclization; Kinetics; Further Variations:Temperatures;
参考文献
Fedorova, Olga A.; Strokach, Yuri P.; Gromov, Sergey P.; Koshkin, Alexander V.; Valova, Tatjana M.; Alfimov, Michael V.; Feofanov, Alexei V.; Alaverdian, Iouri S.; Lokshin, Vladimir A.; Samat, Andre; Guglielmetti, Robert; Girling, Reuben B.; Moore, John N.; Hester, Ronald E.
New Journal of Chemistry, 2002 , vol. 26, # 9 p. 1137 - 1145
反应条件
2,3-bornanedione in toluene also without CQ; Rate constant;
参考文献
Bohne, C.; Fan, M. G.; Li, Z. J.; Lusztyk, J.; Scaiano, J. C.
Journal of the Chemical Society, Chemical Communications, 1990 , # 7 p. 571 - 572
反应条件
in acetonitrile T=13°C; Irradiationphotodecomposition and singlet oxygen production during photosensitization; Product distribution;
参考文献
Salemi-Delvaux, Christiane; Luccioni-Houze, Barbara; Baillet, Gilles; Giusti, Gerard; Guglielmetti, Robert
Tetrahedron Letters, 1996 , vol. 37, # 29 p. 5127 - 5130
反应条件
oxygen in acetonitrile Irradiationsinglet oxygen quenching rate constant in CH2Cl2 at 25 deg C; Mechanism;
参考文献
Baillet, Gilles; Giusti, Gerard; Guglielmetti, Robert
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 4 p. 1220 - 1225
