2,4-二(氯甲基)-1-甲基苯合成路线 (共 6 条)
反应条件
hydrogenchloride; [emim][PF6] T=70°C; 5 h; Ionic liquid;
参考文献
Wang, Yun; Shang, Zhi-Cai; Wu, Tian-Xing
Synthetic Communications, 2006 , vol. 36, # 20 p. 3053 - 3059
反应条件
hydrogenchloride; zinc(II) chloride
参考文献
Drechsler,G.
Journal fuer Praktische Chemie (Leipzig), 1963 , vol. 19, p. 283 - 302
参考文献
Sommelet
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1925 , vol. 180, p. 1350
反应条件
hydrogenchloride 2 h; Heating; Further byproducts. Title compound not separated from byproducts.;
参考文献
Zenkevich; Makarov
Russian Journal of General Chemistry, 2007 , vol. 77, # 4 p. 611 - 619
反应条件
(i) hexamethylenetetramine, aq. AcOH, (ii) aq. HCl; Multistep reaction;
参考文献
Glotzmann,C.
Monatshefte fuer Chemie, 1975 , vol. 106, p. 763 - 777
反应条件
hydrogenchloride; thionyl chloride; zinc(II) chloride in tetrachloromethane
参考文献
Drechsler,G.; Kuehling,H.
Journal fuer Praktische Chemie (Leipzig), 1964 , vol. 23, p. 248 - 258