2-乙基-3-甲基-喹啉合成路线 (共 54 条)
反应条件
carbon monoxide; dicobalt octacarbonyl in tetrahydrofuran
T=105°C; P=760.051 Torr; 48 h;
参考文献
Li, Ng; Jones, William D.
Journal of the American Chemical Society, 2007 , vol. 129, # 35 p. 10707 - 10713
反应条件
benzophenone; potassium tert-butylate in 1,4-dioxane
T=90°C; Friedlaender synthesis; 0.5 h; Inert atmosphere;
参考文献
Martinez, Ricardo; Ramon, Diego J.; Yus, Miguel
Journal of Organic Chemistry, 2008 , vol. 73, # 24 p. 9778 - 9780
反应条件
magnetite-palladium-graphene nanocomposite in acetonitrile
T=80°C; 8.5 h;
参考文献
Verma, Sanny; Verma, Deepak; Jain, Suman L.
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2406 - 2409
反应条件
potassium hydroxide; benzophenone; cis-[RuCl2(dimethylsulfoxide-S)3(dimethylsulfoxide-O)] in 1,4-dioxane
T=80°C; 168 h;
参考文献
Martinez, Ricardo; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 2006 , vol. 62, # 38 p. 8982 - 8987
反应条件
1: allyl bromide With NaCo(CO)4 in tetrahydrofuran
T=20°C;
2: N-vinylmethylphenylamine With carbon monoxide in tetrahydrofuran
T=105°C; P=760.051 Torr; Further stages.;
参考文献
Li, Ng; Jones, William D.
Journal of the American Chemical Society, 2007 , vol. 129, # 35 p. 10707 - 10713
反应条件
palladium on activated charcoal in tetrahydrofuran
T=170°C; 1.5 h; Microwave irradiation;
参考文献
Linciano, Pasquale; Pizzetti, Marianna; Porcheddu, Andrea; Taddei, Maurizio
Synlett, 2013 , vol. 24, # 17 p. 2249 - 2254
反应条件
12-molybdophosphoric acid HPMo; hydrazine hydrate in water
T=40 - 50°C; 2.5 h; regioselective reaction;
参考文献
Hekmatshoar, Rahim; Sajadi, Sodeh; Sadjadi, Samaheh; Heravi, Majid M.; Beheshtiha, Yahya S.; Bamoharram, Fatemeh F.
Journal of the Chinese Chemical Society, 2008 , vol. 55, # 6 p. 1195 - 1198
反应条件
bis(bicyclo[2.2.1]hepta-2,5-diene)dichlorodirhodium; nitrobenzene in ethanol
T=180°C; 4 h;
参考文献
Watanabe, Yoshihisa; Shim, Sang Chul; Mitsudo, Take-aki
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3460 - 3465
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in 1,4-dioxane; water
T=120°C; cyclocondensation; 20 h;
参考文献
Cho, Chan Sik; Kim, Joon Seok; Oh, Byoung Ho; Kim, Tae-Jeong; Shim, Sang Chul; Yoon, Nam Sik
Tetrahedron, 2000 , vol. 56, # 39 p. 7747 - 7750
反应条件
FeCl3*6H2O in tetrachloromethane
T=140°C; 4 h; AutoclaveInert atmosphereSealed tube;
参考文献
Khusnutdinov; Bayguzina; Aminov
Russian Chemical Bulletin, 2013 , vol. 62, # 1 p. 133 - 137
Izv. Akad. Nauk, Ser. Khim., 2013 , # 1 p. 134 - 138