2-乙基-3-甲基-喹啉合成路线 (共 54 条)
反应条件
ruthenium trichloride; bis(1,1-diphenylphosphino)methane; tin(ll) chloride in 1,4-dioxane
T=180°C; 20 h;
参考文献
Chan Sik Cho; Byoung Ho Oh; Sang Chul Shim; Dae Hee Oh
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1315 - 1320
反应条件
dicobalt octacarbonyl; carbon monoxide in tetrahydrofuran
T=95°C;
参考文献
Jacob, Josemon; Jones, William D.
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3563 - 3568
反应条件
air; [IrHCl2(cod)]2 in dimethyl sulfoxide
T=90°C; 12 h;
参考文献
Nakajima, Takayuki; Inada, Takashi; Igarashi, Takeyuki; Sekioka, Tadashi; Shimizu, Isao
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 12 p. 1941 - 1949
反应条件
1: With hydrogenchloride in water
5 h; Reflux;
2: With sodium hydroxide in water; ethyl acetate
T=20°C;
参考文献
Wang, Da-Wei; Wang, Xiao-Bing; Wang, Duo-Sheng; Lu, Sheng-Mei; Zhou, Yong-Gui; Li, Yu-Xue
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2780 - 2787
反应条件
lithium tert-butylate in toluene
T=110°C; 24 h; Inert atmosphere;
参考文献
Liang, Yu-Feng; Zhou, Xin-Feng; Tang, Shi-Ya; Huang, Yao-Bing; Feng, Yi-Si; Xu, Hua-Jian
RSC Advances, 2013 , vol. 3, # 21 p. 7739 - 7742
反应条件
hydrogen; palladium on activated charcoal
参考文献
Familoni, Oluwole B.; Klaas, Phindile J.; Lobb, Kevin A.; Pakade, Vusumzi E.; Kaye, Perry T.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 21 p. 3960 - 3965
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in toluene
T=180°C; 20 h;
参考文献
Cho, Chan Sik; Lee, Na Young; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 3 p. 423 - 429
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in toluene
T=180°C; 20 h;
参考文献
Cho, Chan Sik; Lee, Na Young; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 3 p. 423 - 429
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in 1,4-dioxane; water
T=120°C; cyclocondensation; 20 h;
参考文献
Cho, Chan Sik; Kim, Joon Seok; Oh, Byoung Ho; Kim, Tae-Jeong; Shim, Sang Chul; Yoon, Nam Sik
Tetrahedron, 2000 , vol. 56, # 39 p. 7747 - 7750
反应条件
1: DABCO / CHCl3
2: H2 / 10percent Pd/C / ethanol
View Scheme
参考文献
Familoni, Oluwole B.; Kaye, Perry T.; Klaas, Phindile J.
Chemical Communications, 1998 , # 23 p. 2563 - 2564