2-乙基-3-甲基-喹啉合成路线 (共 54 条)
反应条件
1: DABCO / CHCl3
2: H2 / 10percent Pd/C / ethanol
View Scheme
参考文献
Familoni, Oluwole B.; Kaye, Perry T.; Klaas, Phindile J.
Chemical Communications, 1998 , # 23 p. 2563 - 2564
反应条件
ruthenium trichloride
T=180°C; 4 h;
参考文献
Watanabe, Yoshihisa; Tsuji, Yasushi
Heterocycles, 1984 , vol. 21, # 2 p. 567
反应条件
ruthenium trichloride; bis(1,1-diphenylphosphino)methane; tin(ll) chloride in 1,4-dioxane
T=180°C; 20 h;
参考文献
Chan Sik Cho; Byoung Ho Oh; Sang Chul Shim; Dae Hee Oh
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1315 - 1320
反应条件
tris(triphenylphosphine)ruthenium(II) chloride
T=180°C; 5 h;
参考文献
Watanabe, Yoshihisa; Tsuji, Yasushi
Heterocycles, 1984 , vol. 21, # 2 p. 567
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in 1,4-dioxane
T=180°C; 20 h;
参考文献
Cho, Chan Sik; Lee, Na Young; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 3 p. 423 - 429
反应条件
in tetrahydrofuran
Heating;
参考文献
Katritzky, Alan R.; Arend, Michael
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9989 - 9991
反应条件
zinc dibromide in chloroform
T=90 - 100°C; 2 h; Yield given;
参考文献
Koyama, Junko; Toyokuni, Izumi; Tagahara, Kiyoshi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 332 - 334
反应条件
ruthenium trichloride; triphenylphosphine in 1,4-dioxane
T=180°C; 20 h; Yield given;
参考文献
Cho, Chan Sik; Oh, Byoung Ho; Shim, Sang Chul
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1499 - 1500
反应条件
1: in chloroform-d1
T=50°C;
2: With sodium hydroxide in chloroform-d1; water
参考文献
Vicente, Jose; Chicote, Maria Teresa; Martinez-Martinez, Antonio Jesus
Tetrahedron Letters, 2011 , vol. 52, # 47 p. 6298 - 6302
反应条件
1-hexene; bis(1,1-diphenylphosphino)methane; tin(ll) chloride; ruthenium trichloride in 1,4-dioxane
T=180°C; Cyclization; Alkylation; 20 h; Product distribution; Further Variations:Reagents;
参考文献
Cho, Chan Sik; Oh, Byoung Ho; Kim, Joon Seok; Kim, Tae-Jeong; Shim, Sang Chul
Chemical Communications (Cambridge, United Kingdom), 2000 , # 19 p. 1885 - 1886