甲基(3-氧代丙基)氨基甲酸叔丁酯合成路线 （共 3 条）
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78 - 0°C; Swern oxidation;
参考文献
Xiao, Xiangshu; Antony, Smitha; Kohlhagen, Glenda; Pommier, Yves; Cushman, Mark
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 19 p. 5147 - 5160
反应条件
1: 93 percent / NaH 2: 79 percent / DIBAL-H 3: DMSO; NEt3; (COCl)2 View Scheme
参考文献
Bischoff, Roland; Hamilton, Deborah J.; Jobson, Nicola K.; Sutherland, Andrew
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 323 - 326
反应条件
1: 79 percent / DIBAL-H 2: DMSO; NEt3; (COCl)2 View Scheme
参考文献
Bischoff, Roland; Hamilton, Deborah J.; Jobson, Nicola K.; Sutherland, Andrew
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 323 - 326
