5-氯-2-苯并恶唑羧酸甲酯合成路线 （共 9 条）
反应条件
1: carbon dioxide; 5-chlorobenzo[d]oxazole With caesium carbonate in N,N-dimethyl-formamide T=125°C; P=1064.07 Torr; 16 h; 2: methyl iodide in N,N-dimethyl-formamide Heating;
参考文献
Vechorkin, Oleg; Hirt, Nathalie; Hu, Xile
Organic Letters, 2010 , vol. 12, # 15 p. 3567 - 3569
反应条件
1: C27H37ClCuN3; potassium tert-butylate / tetrahydrofuran / 8 h / 80 °C / 760.05 Torr / Inert atmosphere; sealed tube 2: N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere; sealed tube View Scheme
参考文献
Inomata, Hiroshi; Ogata, Kenichi; Fukuzawa, Shin-Ichi; Hou, Zhaomin
Organic Letters, 2012 , vol. 14, # 15 p. 3986 - 3989
反应条件
Cu(4-Clqo)2 in methanol Heating;
参考文献
Barjesteh, H.; Brain, E. G.; Charalambous, J.; Gaganatsou, P.; Thomas, T. A.
Journal of Chemical Research, Miniprint, 1995 , # 11 p. 2701 - 2720
反应条件
in N,N-dimethyl-formamide T=80°C; 1 h; Inert atmospheresealed tube;
参考文献
Inomata, Hiroshi; Ogata, Kenichi; Fukuzawa, Shin-Ichi; Hou, Zhaomin
Organic Letters, 2012 , vol. 14, # 15 p. 3986 - 3989
参考文献
Musser, J. H.; Hudec, T. T.; Bailey, K.
Synthetic Communications, 1984 , vol. 14, # 10 p. 947 - 954
反应条件
1: dimethylsulfoxide; propan-2-ol 2: K2CO3 3: aq. HCl View Scheme
参考文献
Moeller,H.
Justus Liebigs Annalen der Chemie, 1971 , vol. 749, p. 1 - 11
参考文献
Moeller,H.
Justus Liebigs Annalen der Chemie, 1971 , vol. 749, p. 1 - 11
反应条件
in methanol 1 h; Heating;
参考文献
Castellani, Carla Bisi; Millini, Roberto
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1461 - 1462
反应条件
1: K2CO3 2: aq. HCl View Scheme
参考文献
Moeller,H.
Justus Liebigs Annalen der Chemie, 1971 , vol. 749, p. 1 - 11
