hydrogenchloride in neat (no solvent) under N2 atm. to suspn. anhyd. SnCl2 in butylacrylate added anhyd. HCl during 2 h, temp. maintained at 20°C or below; react. mixt. kept at 150°C/4 mm Hg to remove unreacted butylacrylate and ClCH2CH2COOBu, residue filtered; elem. anal.;
参考文献
Garad, M. V.
Inorganica Chimica Acta, 1984 , vol. 87, p. 79 - 82
Moureu; Murat; Tampier
Annales de Chimie (Cachan, France), 1921 , vol. <9>15, p. 246
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1921 , vol. 172, p. 1269
Khairullin,V.K. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1970 , p. 817 - 821
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1970 , p. 871 - 876
Moureu; Murat; Tampier
Annales de Chimie (Cachan, France), 1921 , vol. <9>15, p. 246
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1921 , vol. 172, p. 1269
