N,4'-二甲基甲酰苯胺合成路线 （共 39 条）
反应条件
water Heating; Yield given;
参考文献
Nippon Shinyaku Co., Ltd.
Patent: EP1452525 A1, 2004 ;
Location in patent: Page 11-12 ;
反应条件
tetrahydrofuran; palladium diacetate in acetic acid
T=40°C; 23 h; Yield given. Yields of byproduct given;
参考文献
Sakakibara,T.; Karasumara,S.; Kawano,I.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6417
反应条件
TEMPO; oxygen in acetonitrile
T=50°C; P=760.051 Torr; 13 h;
参考文献
Song, Ren-Jie; Liu, Yu; Hu, Rui-Xiang; Liu, Yan-Yun; Wu, Ji-Cheng; Yang, Xu-Heng; Li, Jin-Heng
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1467 - 1473
反应条件
chlorhexidine diphosphanilate in acetonitrile
T=100°C; 48 h; Further byproducts given;
参考文献
Humphreys, Robert W. R.
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1483 - 1487
参考文献
Nippon Shinyaku Co., Ltd.
Patent: EP1156045 A1, 2001 ;
Title/Abstract Full Text Show Details
Nippon Shinyaku Co., Ltd.
Patent: EP1243268 A1, 2002 ;
反应条件
tetrahydrofuran; iodobenzene; palladium diacetate
T=50°C; 5 h; Yield given;
参考文献
Sakakibara,T.; Karasumara,S.; Kawano,I.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6417
反应条件
sodium hydroxide in ethanol; water
T=27°C; 9 h;
参考文献
Preedasuriyachai, Patcharee; Kitahara, Hiroaki; Chavasiri, Warinthorn; Sakurai, Hidehiro
Chemistry Letters, 2010 , vol. 39, # 11 p. 1174 - 1176
反应条件
tetrahydrofuran; iodobenzene; palladium diacetate
T=50°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Sakakibara,T.; Karasumara,S.; Kawano,I.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6417
反应条件
[Cu8(H){S2P(OiPr)2}6](PF6); caesium carbonate in N,N-dimethyl-formamide
T=120°C; Ullmann-Goldberg type coupling; 24 h;
参考文献
Wu, Cheng-Chieh; Lee, Bo-Han; Liao, Ping-Kuei; Fang, Ching-Shiang; Liu
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 480 - 484
反应条件
iodobenzene; palladium diacetate
T=50°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Sakakibara,T.; Karasumara,S.; Kawano,I.
Journal of the American Chemical Society, 1985 , vol. 107, p. 6417
