N,4'-二甲基甲酰苯胺合成路线 (共 39 条)
反应条件
oxygen in acetonitrile
T=60°C; 20 h;
参考文献
Murata, Satoru; Tamatani, Akira; Suzuki, Kaoru; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1990 , # 5 p. 757 - 760
反应条件
oxygen in acetonitrile
T=30°C; P=760 Torr; 4 h; other aromatic and aliphatic tert. amines, other anhydrides, other reaction times, influence of BHT, (effect of concentration of) other metal chlorides, effect of anhydride concentration; Product distributionMechanism;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
Benzoyl cyanide; oxygen; copper(l) chloride in acetonitrile
T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298
反应条件
tert.-butylhydroperoxide; orthophosphorus acid; iron(II) chloride in methanol; decane
18.0833 h; Inert atmosphereHeating;
参考文献
Han, Wei; Mayer, Peter; Ofial, Armin R.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1667 - 1676
反应条件
oxygen in acetonitrile
T=30°C; P=760 Torr; 4 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
copper(II) bis(trifluoromethanesulfonate); 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in 1,2-dichloro-ethane
T=20 - 90°C; 14 h; Inert atmosphere;
参考文献
Lv, Yunhe; Zheng, Yiying; Li, Yan; Xiong, Tao; Zhang, Jingping; Liu, Qun; Zhang, Qian
Chemical Communications, 2013 , vol. 49, # 78 p. 8866 - 8868
反应条件
oxygen in acetonitrile
T=30°C; P=760 Torr; 4 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
oxygen in acetonitrile
T=30°C; P=760 Torr; 4 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
oxygen in acetonitrile
T=30°C; P=760 Torr; 4 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
oxygen; iron(III) chloride in acetonitrile
T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298