4-羟基-3-甲氧基苯基-1-丙烷-1,2-二醇合成路线 （共 5 条）
反应条件
sulfuric acid in dichloromethane T=25°C; Hydrolysis;
参考文献
Kikuzaki, Hiroe; Hara, Sanae; Kawai, Yayoi; Nakatani, Nobuji
Phytochemistry, 1999 , vol. 52, # 7 p. 1307 - 1312
反应条件
1: 1.00 g / m-chloroperbenzoic acid / CH2Cl2 / 3 h / 25 °C 2: 228 mg / aq. H2SO4 / CH2Cl2 / 25 °C View Scheme
参考文献
Yadav, Yogesh; Owens, Eric A.; Sharma, Vibhuti; Aneja, Ritu; Henary, Maged
European Journal of Medicinal Chemistry, 2014 , vol. 75, p. 1 - 10
反应条件
1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / acetone; water / 20 °C 2: 5 palladium on charcoal; hydrogen / methanol / 20 °C / |Inert atmosphere View Scheme
参考文献
Yadav, Yogesh; Owens, Eric A.; Sharma, Vibhuti; Aneja, Ritu; Henary, Maged
European Journal of Medicinal Chemistry, 2014 , vol. 75, p. 1 - 10
反应条件
formic acid; dihydrogen peroxide Erwaermen des Reaktionsprodukts mit wss.-methanol. KOH;
参考文献
Ferron; L'Ecuyer
Canadian Journal of Chemistry, 1955 , vol. 33, p. 102,104
反应条件
potassium carbonate in acetone
T=20°C; Methylation;
参考文献
Kikuzaki, Hiroe; Hara, Sanae; Kawai, Yayoi; Nakatani, Nobuji
Phytochemistry, 1999 , vol. 52, # 7 p. 1307 - 1312
