反应条件
Wilkinson's catalyst in toluene
(N2), RhCl(PPh3)3 (5 molpercent) in toluene added to (E)-2(p-toluenethio)styrene in toluene, treated dropwise with catecholborane (L:B=1.1.5), reactedat room temp. for 24 h; evapd.(vac.), dissolved (hexane), stored at -30°C, recrystd. twice (hexane);
参考文献
Webb, Jonathan D.; Harrison, Daniel J.; Norman, David W.; Blacquiere, Johanna M.; Vogels, Christopher M.; Decken, Andreas; Bates, Craig G.; Venkataraman; Baker, R. Thomas; Westcott, Stephen A.
Journal of Molecular Catalysis A: Chemical, 2007 , vol. 275, # 1-2 p. 91 - 100
