1,3-苯并间二氧杂环戊烯合成路线 （共 145 条）
反应条件
N-iodo-succinimide in various solvent(s) T=27°C; 0.416667 h;
参考文献
Yadav; Reddy; Basak; Narsaiah
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 1 p. 77 - 82
参考文献
Ortho Pharmaceutical Corporation
Patent: US4761413 A1, 1988 ;
US 4761413 A
反应条件
T=150°C; anschl. mit methanol. KOH;
参考文献
Johnson et al.
Journal of the Chemical Society, 1953 , p. 2136,2138
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide; benzene 24 h; Heating;
参考文献
Melis, Stefana; Monni, Francesca; Piras, Pier Paolo; Sotgiu, Francesca
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 463
反应条件
sodium iodide in acetonitrile 6 h; Ambient temperature; Product distribution;
参考文献
Corda, Luciana; Fadda, Anna Maria; Maccioni, Antonio; Maccioni, Anna Maria; Podda, Gianni
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 311 - 314
反应条件
sulfuric acid; hydroxylamine-o-sulphonic acid; iron(II) sulfate in water; N,N-dimethyl-formamide T=30 - 35°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Citterio, Attilio; Gentile, Anna; Minisci, Francesco; Navarrini, Valter; Serravalle, Marco; Ventura, Susanna
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4479 - 4482
反应条件
1: Methylenedioxybenzene With sulfur trioxide-N,N-dimethylformamide complex in anhydrous dichloroethane T=75°C; 22.0833 h; 2: oxalyl dichloride in anhydrous dichloroethane T=26 - 67°C; 6.5 h;
参考文献
G. D. Searle and Co.
Patent: US6388132 B1, 2002 ;
Location in patent: Page column 52 ;
反应条件
sulfuryl dichloride in hexane; dichloromethane; N,N-dimethyl-formamide
参考文献
G.D. Searle and Co.
Patent: US5985870 A1, 1999 ;
US 5985870 A
反应条件
thionyl chloride in water; ethyl acetate
参考文献
Eli Lilly and Company
Patent: US5387681 A1, 1995 ;
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide; benzene 24 h; Heating;
参考文献
Melis, Stefana; Monni, Francesca; Piras, Pier Paolo; Sotgiu, Francesca
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 463
