1,3-苯并间二氧杂环戊烯合成路线 (共 145 条)
反应条件
1: chloroform; N-bromo-succinimide 2: pyridine / 220 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 23, p. 908
反应条件
1: With oxygen; sodium acetate; acetylacetone; palladium diacetate in propionic acid T=70°C; P=760.051 Torr; 3 h; 2: With hydrogen; palladium on activated charcoal P=760.051 Torr; Further stages.;
参考文献
Yamada, Tomoyuki; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5471 - 5474
反应条件
1: 71 percent / HBr/AcOH / 0 - 20 °C 2: 98 percent / dimethylformamide / 3 h / Heating 3: 70 percent / EtOLi / ethanol / 8 h / Heating 4: 78 percent / H2 / Pd/C / CHCl3; methanol / 48 h / 20 °C 5: 75 percent / AlBr3; EtSH / 24 h / 20 °C View Scheme
参考文献
Belloni, Maura; Manickam; Wang, Zehn-He; Preece, Jon A.
Molecular Crystals and Liquid Crystals, 2003 , vol. 399, p. 93 - 114
反应条件
ammonium cerium(IV) nitrate; lithium bromide in acetonitrile T=20°C; 2 h;
参考文献
Roy, Subhas Chandra; Guin, Chandrani; Rana, Kalyan Kumar; Maiti, Gourhari
Tetrahedron Letters, 2001 , vol. 42, # 39 p. 6941 - 6942
参考文献
US2014/128392 A1, ;
Page/Page column ;
参考文献
Gensler; Stouffer
Journal of Organic Chemistry, 1958 , vol. 23, p. 908
反应条件
nitric acid in acetic acid
参考文献
Hoffmann-La Roche Inc.
Patent: US4435406 A1, 1984 ;
反应条件
nitric acid T=25°C; 1 h;
参考文献
Takakis, Ioannis M.; Hadjimihalakis, Phaedon M.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 3 p. 625 - 634
反应条件
in dichloromethane T=20°C; 2 h; Irradiation;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola
Acta Chemica Scandinavica, 1997 , vol. 51, # 6-7 p. 718 - 732
反应条件
in ethanol; dichloromethane T=20°C; 10 h; Irradiationvarious solvents; the effects of ethanol, temperature, and reaction time; Product distribution;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola
Acta Chemica Scandinavica, 1997 , vol. 51, # 6-7 p. 718 - 732