1,3-苯并间二氧杂环戊烯合成路线 （共 145 条）
反应条件
1: boron trifluoride diethyl etherate / 1,2-dichloro-ethane / 3.25 h / -5 °C
2: sodium acetate; hydroxylamine hydrochloride / methanol / 2 h / |Reflux
3: sodium hydrogensulfite; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 / 1,2-dichloro-ethane / 12 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Murugan, Kaliyappan; Huang, Da-Wei; Chien, Yu-Ting; Liu, Shiuh-Tzung
Tetrahedron, 2013 , vol. 69, # 1 p. 268 - 273
反应条件
aluminium trichloride; nitrobenzene
参考文献
Podda, G.; Maccioni, A.; Fadda, A.; Daolio, S.; Traldi, P.; Vecchi, E.
Organic Mass Spectrometry, 1983 , vol. 18, # 7 p. 318 - 320
参考文献
Haworth; Kelly
Journal of the Chemical Society, 1936 , p. 745
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=150°C; 2 h;
参考文献
Imakura; Okimoto; Konishi; Hisazumi; Yamazaki; Kobayashi; Yamashita
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 7 p. 1691 - 1696
反应条件
1: 80 percent / acetic acid / 1 h / Ambient temperature
2: 84 percent / sodium bis(methoxyethoxy)aluminum dihydride / benzene / 0.75 h / 5 - 10 °C
View Scheme
参考文献
Ruffin, L. D.; Bowlus, S. B.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 461 - 462
