1,3-苯并间二氧杂环戊烯合成路线 （共 145 条）
反应条件
hydrogenchloride; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; 4-nitroso-N,N-di-methylaniline Reagens 4: Zinkchlorid, Erwaermen des Reaktionsgemisches mit Wasser;
参考文献
Schorygin et al.
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 975,978
Chem. Zentralbl., 1939 , vol. 110, # I p. 2178
反应条件
hydrogenchloride in water; toluene T=20 - 25°C; 4 h; Conversion of starting material;
参考文献
ENDURA S.P.A.
Patent: WO2005/42512 A1, 2005 ;
Location in patent: Page/Page column 8 ;
反应条件
formaldehyd; zinc(II) chloride; Petroleum ether Reagens 4: Chlorwasserstoff;
参考文献
Schorygin et al.
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 975,978
Chem. Zentralbl., 1939 , vol. 110, # I p. 2178
参考文献
Schorygin et al.
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 975,978
Chem. Zentralbl., 1939 , vol. 110, # I p. 2178
反应条件
tin(IV) chloride in dichloromethane T=20°C; 1 h;
参考文献
Daukshas, V. K.; Gaidyalis, P. G.; Pyatrauskas, O. Yu.; Udrenaite, E. B.; Gasperavichene, G. A.; Raguotene, N. V.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 5 p. 341 - 345
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 5 p. 569 - 573
反应条件
perchloric acid T=0 - 20°C; 3 h;
参考文献
Endura S.p.A.
Patent: US6342613 B1, 2002 ;
Location in patent: Page column 6 ;
反应条件
tetrachloromethane; di-tert-butyl peroxide in benzene T=130°C; 2 h;
参考文献
Sokolovskii, A. V.; Nazarov, D. V.; Rol'nik, L. Z.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 6 p. 1305 - 1308,1159 - 1162
反应条件
dihydrogen peroxide; titanium-silicalite catalyst (TS-1) in isobutyl methylketone; acetone T=60°C; 5 h; Conversion of starting material;
参考文献
BORREGAARD ITALIA S.P.A.
Patent: WO2004/14827 A1, 2004 ;
Location in patent: Page 9 ;
反应条件
1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione in acetic acid T=60 - 95°C; 1 h; Product distribution / selectivity;
参考文献
UBE INDUSTRIES, LTD.
Patent: WO2007/20964 A1, 2007 ;
Location in patent: Page/Page column 10-11 ;
反应条件
chlorine; acetic acid
参考文献
Orr; Robinson; Williams
Journal of the Chemical Society, 1917 , vol. 111, p. 948
