1: With sulfuryl dichloride in tetrahydrofuran
T=0 - 20°C; 18 h; Inert atmosphere;
2: With oxygen in tetrahydrofuran
0.5 h;
参考文献
THE REGENTS OF THE UNIVERSITY OF MICHIGAN; Neubig, Richard; Blazer, Levi; Husbands, Stephen; Larsen, Scott; Traynor, John
Patent: US2012/277273 A1, 2012 ;
Location in patent: Page/Page column 22-23 ;