2-(丙基硫基)-1,3-苯并噻唑合成路线 (共 12 条)
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=0°C; Mitsunobu substitution;
参考文献
Sorg, Achim; Brueckner, Reinhard
Synlett, 2005 , # 2 art. no. G39004ST, p. 289 - 293
反应条件
N-ethyl-N,N-diisopropylamine in acetone T=20°C; 0.333333 h; Sonication;
参考文献
Deligeorgiev, Todor; Kaloyanova, Stefka; Lesev, Nedyalko; Vaquero, Juan J.
Ultrasonics Sonochemistry, 2010 , vol. 17, # 5 p. 783 - 788
反应条件
potassium carbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=50°C; 5 h;
参考文献
Hu, Yi; Chen, Zhen-Chu; Le, Zhang-Gao; Zheng, Qin-Guo
Synthetic Communications, 2004 , vol. 34, # 11 p. 2039 - 2046
反应条件
[2,2']bipyridinyl; copper(l) iodide; oxygen; sodium carbonate in N,N-dimethyl-formamide T=140°C; 24 h;
参考文献
Ranjit, Sadananda; Lee, Richmond; Heryadi, Dodi; Shen, Chao; Wu, Ji'En; Zhang, Pengfei; Huang, Kuo-Wei; Liu, Xiaogang
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8999 - 9007
反应条件
1: carbon disulfide; propane-1-thiol With potassium carbonate in N,N-dimethyl-formamide T=20°C; 1 h; 2: 2-iodo aniline With copper(I) bromide in N,N-dimethyl-formamide T=110°C; 6 h;
参考文献
Shi, Liu; Liu, Xiangqian; Zhang, Hui; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 4200 - 4204
反应条件
sodium hydroxide; Amberlite IRA-400 chloride form in water; acetone
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 539 - 546
反应条件
in 1,4-dioxane T=20°C; 0.166667 h;
参考文献
Yu, Yanfei; Li, Zhengning; Jiang, Lan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 632 - 640
参考文献
Dou,H.J.M. et al.
Helvetica Chimica Acta, 1978 , vol. 61, p. 3143 - 3148
反应条件
in tetrahydrofuran Alkylation; Heating;
参考文献
Harizi, Abdallah; Romdhane, Anis; Mighri, Zine
Tetrahedron Letters, 2000 , vol. 41, # 31 p. 5833 - 5835
反应条件
in N,N-dimethyl-formamide T=20°C; 3 h;
参考文献
Ghosh, Arun K.; Zajc, Barbara
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8531 - 8540