4-溴-2’-甲氧基苯甲酮合成路线 （共 4 条）
反应条件
chromium(VI) oxide; sulfuric acid in acetone T=20°C; Jones oxidation; 0.166667 h;
参考文献
Revesz, Laszlo; Blum, Ernst; Di Padova, Franco E.; Buhl, Thomas; Feifel, Roland; Gram, Hermann; Hiestand, Peter; Manning, Ute; Rucklin, Gerard
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3601 - 3605
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.08 h / -78 °C 1.2: tetrahydrofuran 2.1: CrO3; H2SO4 / acetone / 0.17 h / 20 °C View Scheme
参考文献
Revesz, Laszlo; Blum, Ernst; Di Padova, Franco E.; Buhl, Thomas; Feifel, Roland; Gram, Hermann; Hiestand, Peter; Manning, Ute; Rucklin, Gerard
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3601 - 3605
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.08 h / -78 °C 1.2: tetrahydrofuran 2.1: CrO3; H2SO4 / acetone / 0.17 h / 20 °C View Scheme
参考文献
Revesz, Laszlo; Blum, Ernst; Di Padova, Franco E.; Buhl, Thomas; Feifel, Roland; Gram, Hermann; Hiestand, Peter; Manning, Ute; Rucklin, Gerard
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3601 - 3605
反应条件
1: With trifluoroacetic anhydride T=80°C; 2: With boron trifluoride diethyl etherate T=80°C; Friedel-Crafts reaction; Title compound not separated from byproducts;
参考文献
Wilkinson, Mark C.; Saez, Fabienne; Wei, Lee Hon
Synlett, 2006 , # 7 p. 1063 - 1066
